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IN THIS CHAPTER Summary: The free-response portion of the AP exam will contain a question concerning an experiment, and there may also be a few multiple-choice questions on one or more of these experiments This chapter reviews the basic experiments that the AP Exam Committee believes to be important You should look over all of the experiments in this chapter and pay particular attention to any experiments you did not perform In some cases you may find, after reading the description, that you did a similar experiment Not every AP class does every experiment, but any of these experiments may appear on the AP exam The free-response questions on recent exams have been concerned with the equipment, measurements, and calculations required In some cases, sources of error are considered To answer the question completely, you will need an understanding of the chemical concepts involved To discuss an experiment, you must be familiar with the equipment needed In the keywords section at the beginning of this chapter is a complete list of equipment for the experiments Make sure you are familiar with each item You may know an item by a different name, or you may need to talk to your teacher to get additional information concerning an item In some cases, the exam question will request a list of the equipment needed, while in other cases you will get a list from which to choose the items you need Certain items appear in many experiments These include the analytical balance, beakers, support stands, pipets, test tubes, and Erlenmeyer flasks Burets, graduated cylinders, clamps, desiccators, drying ovens, pH meters, volumetric flasks, and thermometers are also commonly used If you are not sure what equipment to choose, these serve as good guesses Most of the remaining equipment appears in three or fewer experiments
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You will need to know the basic measurements required for the experiment For example, you may need to measure the initial and final temperatures Do not make the mistake of saying you measure the change in temperature
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Experimental 279 You calculate the change in temperature from your measured initial and final temperatures You do not need to give a lot of detail when listing the required measurements, but you need to be very specific in what you measure Many students, have lost exam points for not clearly distinguishing between measured and calculated values The basic calculations fall into two categories Simple calculations, such as the change in temperature or the change in volume, are the easiest to forget Simple calculations may also include mass-to-mole conversions The other calculations normally involve entering values into one of the equations given at the beginning of the previous chapters of this book Beginning with the 2007 AP Chemistry exam, experimental questions may be incorporated into any of the free-response questions This means that you will need to have a good understanding of the experiments in order to discuss not only the experiment itself, but the underlying chemical concepts Therefore, when studying each experiment, refer back to the appropriate material to review the concepts involved Keywords and Equations Pay particular attention to the specific keywords and equation in the chapters associated with the individual experiments
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A = abc (A = absorbance; a = molar absorbtivity; b = path length; c = concentration)
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analytical balance buret capillary tubes crucible and cover drying oven evaporating dish forceps hot plate Meker burner pipet rubber tubing stopwatch test-tube rack triangle crucible support wash bottle wire gauze barometer burner centrifuge cuvettes electrodes filter crucibles and adapters funnel ice mortar and pestle power supply (battery) spectrophotometer support stand thermometer voltmeter watch glass beaker(s) calorimeter clamp desiccator Erlenmeyer flask filter flasks graduated cylinder ion exchange resin or silica gel pH meter Pt or Ni test wire stirrer test tube(s) tongs volumetric flask water bath
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