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8 Adsorption and Ion Exchange
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De nitions Adsorption is separation of the components of a uid phase brought about by contacting the uid phase with a xed solid phase The solid phase, termed the sorbent, consists generally of highly porous particles with greatly extended surface area, most of which is internal One or more components of the uid phase, termed sorbates, enter the sorbent particles and bond to the surface of the solid In physical adsorption, weak forces such as ionic or Van der Waals forces bond sorbate molecules to the surface In chemisorption, true chemical bonds form between sorbate and sorbent surface Molecular sieves possess a large number of adsorption sites of uniform type and essentially molecular dimensions and can be extremely selective toward a given component or class of components Ion exchange is transfer of ions from a uid phase to a solid phase with simultaneous transfer of other similarly charged ions in the reverse direction The solid medium is a synthetic organic resin with functional groups having a given charge bonded to the resin matrix and hence immobile Mobile ions of opposite charge are distributed throughout the matrix to maintain electrical neutrality Cationexchange resins have negatively charged functional groups (such as sulfonic groups)
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CHAPTER FIFTEEN
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bound to the matrix, while anion-exchange resins have positively charged bound groups (quaternary ammonium groups in strongly basic resins and other amine groups in weakly basic resins) If the mobile ion X is predominant, the resin is said to be in the X form (eg, if Cl ions are the predominant mobile ion, the resin is in chloride form) Once the sorbent has become saturated, the sorbate is stripped from the sorbent and recovered, returning the sorbent to its original condition for reuse This is termed regeneration and may be accomplished by heating, chemical reaction, or contacting with a regenerant Design Design for continuous operation generally depends on scale-up from an experimentally determined breakthrough curve for a particular sorbent-sorbate uid system It is generally found that for a given system the ratio of ef uent concentration is a function of the quantity of liquid treated (expressed as volumes of liquid per volume of solid, dimensionless), residence time, and effective mass-transfer rate For a given system at a given set of equilibrium conditions, the same functional relationship must hold: X F aV DbF p
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b where F a / D p is a dimensional group controlling mass-transfer rate, V / F is the residence time, and (v / V ) is the total throughput in bed volumes If mass transfer is rapid enough to ensure instantaneous equilibrium at all points, the effects of the mass-transfer parameter and residence time are not signi cant, and
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The shape of this curve is dependent on equilibrium considerations only (ie, the feed concentration and the adsorption isotherm)
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9 Membrane Processes Several diffusional separation processes involve transfer of one or more components from one uid phase through a porous solid medium or membrane to a second uid phase The porous medium, generally very thin, does not permit ow of the uid but does allow the transfer of material between phases by molecular diffusion through pores Membrane processes are classi ed according to the driving force across the membrane causing this diffusion; in membrane permeation, the driving force is a difference in partial pressure; in dialysis, the driving force is a concentration difference; in ultra ltration and reverse osmosis, the driving force is a difference in pressure; and in electrodialysis, the driving force is a voltage gradient
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Membrane Permeation For steady-state processes the rate of permeation of a component through the membrane is given by NM where P ( p) L (1534)
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