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Sampling Technique After determining from the velocity traverse that the sampling location is suitable, the diameter of the sampling probe tip and the desired sampling rate must be selected Isokinetic sampling means sampling with the same inlet velocity at the probe tip as the owing gas stream has at the same site Sampling isokinetically is necessary to obtain a representative sample of large particles Particle-Size Measurement Particle-size measurements are usually made either by laboratory analysis or by classi cation into various size ranges in a owing gas sample Where an unclassi ed sample is collected, particle size is usually measured by microscopic measurement or resuspension and classi cation in either an air stream or a liquid With microscopic methods, a thin deposit of solids may be collected on a dry membrane lter or a glass slide using an electrostatic or thermal precipitator sampler The sizes of particles are measured visually, and the number in each size range is counted The particles are usually measured by equivalent area or by a predominant dimension To obtain particle-size distribution on a mass basis, it is necessary to make assumptions about particle volume and density Monitoring For monitoring pollutant gases, a number of instruments have been developed using infrared and ultraviolet absorption These are adaptable to SO2, NO, CO, CO2, hydrocarbons, and other speci c gases Membrane-type cells involving oxidation-reduction reactions with the pollutant also have been developed There is a need to predict plume opacity for compliance with regulations when certain particulate collection ef ciencies are anticipated or speci ed Ensor and Pilat29 present a theoretical equation for relating plume opacity and particle concentration and properties: W where W I/ I0 L K K ln (I/ I0) L (1586)
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the particle mass concentration, g / m3 true particle density, g / cm3 ratio of light transmitted through plume to quantity transmitted if there were no emission [opacity 1 (I / I0)] length of light path, m a proportionality constant, cm3 / m2, and dependent on particle properties and light wavelength
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This equation is most accurate for a process in which particle-size distribution is constant and when the value of K has been determined experimentally by measuring opacity and particle concentration simultaneously However, predictions of plume opacity can be made with fair accuracy from fundamental data on the mass-median particle size, the standard particle-size deviation, the density of the particles, and their refractive index Theoretical values of K are given in Ensor and Pilat29
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Minimizing Need for Collection Devices There are several means of reducing or eliminating pollutants without speci c removal devices Examples are substitution of low-sulfur fuels, nonvolatile solvents, operation at lower temperatures to reduce NOx formation or volatilization of a processed material; use of indirect rather than direct-contact heat transfer; heat transfer from radiant panels; pretreatment of nat-
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ural raw materials to remove easily airborne nes or volatiles; and wetting or agglomeration of solids to reduce airborne releases during handling Application of Control Devices Table 154 lists equipment types useful for reducing emission of gases, odors, and particulates Some odors can be canceled by other antagonistic odor molecules This provides a means of eliminating an odor without actually preventing its release
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Absorption This is one of the most frequently used methods for removal of watersoluble gases Acidic gases (such as HCl, HF, and SIF4) can readily be absorbed in water ef ciently, especially if contact is with water having an alkaline pH Lesssoluble acidic gases (such as SO2, Cl2, and H2S) can be absorbed more readily in a dilute caustic solution such as 5 to 10 percent NaOH Scrubbing with an ammonium salt solution is also employed; the gas is often contacted with the more alkaline solution rst and a neutral or slightly acid solution last to prevent loss of NH3 to the atmosphere Lime is an inexpensive alkali but often leads to plugging problems in absorption equipment if the calcium salts have only limited solubility A better technique is to absorb with an NaOH solution, which is then limed external to the absorption tower The calcium salts are settled out and the regenerated NaOH returned to the absorption system Adsorption Adsorption processes consist of contacting a gas with a solid The solids are essentially porous with an af nity for certain substances Typical materials are activated carbon, activated alumina, silica gels, and molecular sieves An adsorbent can hold from 8 to 25 percent of its own weight in adsorbed vapors
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